Beilstein J. Nanotechnol.2013,4, 285–291, doi:10.3762/bjnano.4.31
parallelanalysis; ESI-MS; 3D printing; reactionware; supramolecular chemistry; Introduction
Flow chemistry is a growing field that can increase productivity and control, ensure reproducibility and reduce manual handling [1]. There is currently a huge interest in directly interfacing milli- and
of the reactions being recorded continuously and in parallel by ESI-MS. Utilising in-house-programmed computer control, the reactant flow rates and order were carefully controlled and varied, with the changes in the pump inlets being mirrored by the recorded ESI-MS spectra.
Keywords: continuous
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Scheme 1:
Reaction scheme for the formation of the ttop and metal-salt coordination complex (1 is [Cu(C24H24N6...